(N-Benzoyl-N′-phenylthiourea-κS)chlorido(η4-1,5-cyclooctadiene)rhodium(I)
نویسندگان
چکیده
منابع مشابه
N-Benzoyl-N′,N′-dimethylthiourea
In the title compound, C(10)H(12)N(2)OS, the amide NCO group is twisted relative to the thio-ureido SCN(2) group, forming a dihedral angle of 55.3 (2)°. The crystal packing shows inter-molecular N-H⋯S and weak C-H⋯O inter-actions, the former giving rise to the formation of centrosymmetric R(2) (2)(8) dimers.
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In the title compound, C(14)H(12)N(2)O(2), the mol-ecular conformation is determined by a strong intra-molecular N-H⋯O=C hydrogen bond. In the crystal, pairs of mol-ecules are connected by inter-molecular N-H⋯O=C hydrogen bonds, forming centrosymmetric dimers. No specific inter-actions between dimers could be found.
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In the title compound, C(14)H(13)NO(3)S, the conformation of the N-H bond in the C-SO(2)-NH-C(O) segment is anti to the C=O bond. The tolyl and benzoyl groups are twisted about the S-N bond, with a C-S-N-C torsion angle of 68.8 (4)°. The dihedral angle between the sulfonyl and the benzoyl benzene rings is 73.9 (1)°. In the crystal, the mol-ecules are linked into C(4) chains along the c axis by ...
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ژورنال
عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online
سال: 2010
ISSN: 1600-5368
DOI: 10.1107/s1600536810029740